丙环唑,60207-90-1，生产厂家，价格-洛克化工网移动版

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基本信息

制备方法及用途

物化性质

安全信息

毒理性

MSDS

海关数据

结构与计算化学

表征图谱

丙环唑

中文名称：: 丙环唑

中文别名：: 丙环唑;
丙唑灵;
1-[2-(2,4-二氯苯基)-4-丙基-1,3-二氧戊环-2-甲基]-1氢-1,2,4-三唑;
1-[2,4-二氯苯基)-4-丙基-1,3-二氧戊环-2-甲基]-1氢-1,2,4-三唑;
1-[2-(2,4-二氯苯基)-4-丙基-1,3-二氧戊环-α-甲基]-1-氢-1,2,4-三唑;
普克利;
必扑尔;
敌力脱;
氧环三宝25EC;
1-[2-(2,4-二氯苯基)-4-丙基-1,3-二氧戊环-2-基甲基]-1H-1,2,4-三唑

英文名称：: Propiconazole

英文别名：: propiconazole;
DESME;
TRUST;
Propiconazole;
1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl]-1H-1,2,4-triazole;
radar;
Dadar;
orbit;
FORDO;
TILT;
1-{[(2Ξ,4Ξ)-2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl}-1H-1,2,4-triazole;
(2RS,4RS;
JUNO;
desmel;
2RS,4SR)-1-[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-ylmethyl]-1H-1,2,4-triazole

CAS No.：: 60207-90-1

分子式：: C₁₅H₁₇C_l2N₃O₂

分子量：: 342.22

精确分子量：: 341.07000

PSA：: 49.17000

MDL：: MFCD00055299

EINECS：: 262-104-4

BRN：: 9349305

InChI：: InChI=1/C15H17Cl2N3O2/c1-2-3-12-7-21-15(22-12,8-20-10-18-9-19-20)13-5-4-11(16)6-14(13)17/h4-6,9-10,12H,2-3,7-8H2,1H33

危险品标志：: Xn，N，T，F

风险术语：: R22;R43;R50/53;R39/23/24/25;R23/24/25;R11;

安全术语：: S36/37;S46;S60;S61;S45;S16;S7;

分子结构式：

SDS：: 查看

丙环唑制备方法及用途

制备方法

1.先将2，4-二氯苯基甲酮溴化，生成2，4-二氯苯基溴甲基酮。再将2，4-二氯苯基溴甲基酮与1，2-戊二醇在对甲苯磺酸的存在下，于甲苯溶剂中反应生成相应的缩酮。然后在二甲基甲酰胺中与1H-1，2，4-三唑反应，制得丙环唑制备方法二制备方法三

合成制备方法

1.先将2，4-二氯苯基甲酮溴化，生成2，4-二氯苯基溴甲基酮。再将2，4-二氯苯基溴甲基酮与1，2-戊二醇在对甲苯磺酸的存在下，于甲苯溶剂中反应生成相应的缩酮。然后在二甲基甲酰胺中与1H-1，2，4-三唑反应，制得丙环唑

制备方法二

制备方法三

用途简介

具有保护和治疗作用的内吸性三唑类杀菌剂，可被根茎叶部吸收，并很快地在植物体内向上传导。

用途

三唑类内吸性杀菌剂。具有保护和治疗作用，属麦角甾醇生物合成的抑制剂。麦角甾醇在真菌细胞膜的构成中起重要作用，丙环唑通过干扰C14-去甲基化而妨碍真菌体内麦角甾醇的生物合成，从而破坏真菌的生长繁殖，起到保护和治疗作用。丙环唑除对藻菌病害无效外，对子囊菌属、担子菌属、半知菌属真菌在粮食作用、蔬菜、水果以及观赏植物上引起的多种病害有效，特别是对小麦根腐病、白粉病、水稻恶苗病，各种锈病、叶斑病、颖枯病、网黑穗病等，具有较好的防治效果，但对卵茵病害无效。残效期达3～5周。如防治小麦白粉病、条锈病、根腐病，在发病的初期用25%乳油5mL/100m²对水11.25kg喷雾，防治小麦颖枯病则在孕穗期喷雾，防治大麦叶锈病、网斑病、燕麦冠锈病可用同样剂量喷雾。据报道，用于麦类锈病增产显著。防治水稻恶苗病，将25%乳油1000倍浸水稻种子2～3d后直接催芽播种。此外，还可用于黄瓜白粉病、菜豆白粉病、番茄白粉病、苹果白粉病、黑星病、青霉腐料病和花生、大豆、咖啡等多种病害。
丙环唑是一种具有保护和治疗作用的内吸性三唑类杀菌剂，可被根、茎、叶部吸收，并能很快地在植物株体内向上传导，防治子囊菌，担子菌和半知菌引起的病害，特别是对小麦全蚀病、白粉病、锈病、根腐病，水稻恶菌病，香蕉叶斑病具有较好的防治效果。(1)防治麦类病害。(2)防治水稻恶苗病。(3)防治葡萄白粉病、炭疽病。(4)防治花生叶斑病。(5)防治香蕉叶斑病、叶条斑病。

丙环唑物化性质

外观与性状：
通常作为黄色液体供应

密度：
1.39 g/cm3

沸点：
180°C (0.1 torr)

闪点：
11 °C

折射率：
1.623

存储条件/存储方法：
库房通风低温干燥,与食品原料分开储运

稳定性相关：

参与丙酮、甲醇、异丙醇等大多数有机溶剂互溶，对光、热、酸、碱都较稳定，对金属无腐蚀性。对兔眼
睛黏膜和皮肤有轻度刺激，对豚鼠无致敏作用，在试验条件下未见三致现象。

其它信息：

1.       性状：淡黄色黏稠液体
2.       密度（g/cm³ 20ºC）：1.27
3.       相对蒸汽密度（g/mL,空气=1）：未确定
4.       熔点（ºC）：未确定
5.       沸点（ºC）：180
6.       沸点（ºC,5.2kPa）：未确定
7.       折射率（°）：1.5468
8.       闪点（ºC）：11
9.       比旋光度（º）：未确定
10.    自燃点或引燃温度（ºC）：未确定
11.    蒸气压（kPa,20ºC）：0.133×10^-3
12.    饱和蒸气压（kPa,60ºC）：未确定
13.    燃烧热（KJ/mol）：未确定
14.    临界温度（ºC）：未确定
15.    临界压力（KPa）：未确定
16.    油水（辛醇/水）分配系数的对数值（25℃）：未确定
17.    爆炸上限（%,V/V）：未确定
18.    爆炸下限（%,V/V）：未确定
19.    溶解性(mg/L 20ºC)：水：110

丙环唑安全信息

海关代码：
2934999025

危险类别码：
R22

安全说明：
S36/37-S46-S60-S61-S45-S16-S7

RTECS号：
XZ4620000

安全标志：
S40:清理被该物质污染的地面和物体，使用（合适的清洁材料名称）。
S60:本物质残余物和容器必须作为危险废物处理。
S61:避免排放到环境中。参考专门的说明/安全数据表。
:

危险标志：
Xn: Harmful;N: Dangerous for the environment;T: Toxic;F: Flammable;

丙环唑毒理性

CHEMICAL IDENTIFICATION

RTECS NUMBER :
XZ4620000

CHEMICAL NAME :
1H-1,2,4-Triazole, 1-((2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl )methyl)-

CAS REGISTRY NUMBER :
60207-90-1

BEILSTEIN REFERENCE NO. :
0841361

LAST UPDATED :
199710

DATA ITEMS CITED :
7

MOLECULAR FORMULA :
C15-H17-Cl2-N3-O2

MOLECULAR WEIGHT :
342.25
HEALTH HAZARD DATA
ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Rodent - rat

DOSE/DURATION :
1517 mg/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

REFERENCE :
PBCDDQ Proceedings-British Crop Protection Conference-Pests and Diseases. (British Crop., Protection Council, 2A Kidderminster Rd., Croydon, CRO 2UE, UK) 1977- Volume(issue)/page/year: -,508,1979

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Administration onto the skin

SPECIES OBSERVED :
Rodent - rat

DOSE/DURATION :
>4 gm/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

REFERENCE :
PBCDDQ Proceedings-British Crop Protection Conference-Pests and Diseases. (British Crop., Protection Council, 2A Kidderminster Rd., Croydon, CRO 2UE, UK) 1977- Volume(issue)/page/year: -,508,1979 ** OTHER MULTIPLE DOSE TOXICITY DATA **

TYPE OF TEST :
TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Rodent - rat

DOSE/DURATION :
11375 mg/kg/13W-C

TOXIC EFFECTS :
Liver - hepatitis (hepatocellular necrosis), zonal Liver - changes in liver weight Nutritional and Gross Metabolic - weight loss or decreased weight gain

REFERENCE :
TOXID9 Toxicologist. (Soc. of Toxicology, Inc., 475 Wolf Ledge Parkway, Akron, OH 44311) V.1- 1981- Volume(issue)/page/year: 12,118,1992 ** REPRODUCTIVE DATA **

TYPE OF TEST :
TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :
Oral

DOSE :
759 ug/kg

SEX/DURATION :
female 6-15 day(s) after conception

TOXIC EFFECTS :
Reproductive - Fertility - post-implantation mortality (e.g. dead and/or resorbed implants per total number of implants) Reproductive - Effects on Embryo or Fetus - fetotoxicity (except death, e.g., stunted fetus)

REFERENCE :
BFPHA8 Bulletin of the Faculty of Pharmacy (Cairo University). (Faculty of Pharmacy, Cairo Univ., Cairo, Egypt) V.1- 1961/62- Volume(issue)/page/year: 31,459,1993 *** U.S. STANDARDS AND REGULATIONS *** EPA FIFRA 1988 PESTICIDE SUBJECT TO REGISTRATION OR RE-REGISTRATION FEREAC Federal Register. (U.S. Government Printing Office, Supt. of Documents, Washington, DC 20402) V.1- 1936- Volume(issue)/page/year: 54,7740,1989

毒理学数据：

大鼠急性经口LD50>1517mg/kg，急性经皮LD50> 4000mg/kg,鲤鱼LC50 100 mg /L，虹蝉783mg /L(均96h)。

生态数据：

对水是稍微危害的，若无政府许可，勿将材料排入周围环境

丙环唑 MSDS

Section 1. IDENTIFICATION OF THE SUBSTANCE/MIXTURE
  Product identifiers
    Product name        : Propiconazole
    CAS-No.        : 60207-90-1
  Relevant identified uses of the substance or mixture and uses advised against
    Identified uses        : Laboratory chemicals, Manufacture of substances



Section 2. HAZARDS IDENTIFICATION
  Classification of the substance or mixture
  Classification according to Regulation (EC) No 1272/2008 [EU-GHS/CLP]
    Acute toxicity, Oral (Category 4)
    Skin sensitization (Category 1)
    Acute aquatic toxicity (Category 1)
    Chronic aquatic toxicity (Category 1)
  Classification according to EU Directives 67/548/EEC or 1999/45/EC
    Harmful if swallowed. May cause sensitization by skin contact. Very toxic to aquatic organisms, may cause
    long-term adverse effects in the aquatic environment.
  Label elements
  Labelling according Regulation (EC) No 1272/2008 [CLP]
    Pictogram
    Signal word        Warning
    Hazard statement(s)
    H302        Harmful if swallowed.
    H317        May cause an allergic skin reaction.
    H410        Very toxic to aquatic life with long lasting effects.
    Precautionary statement(s)
    P273        Avoid release to the environment.
    P280        Wear protective gloves.
    P501        Dispose of contents/ container to an approved waste disposal plant.
    Supplemental Hazard        none
    Statements
  According to European Directive 67/548/EEC as amended.
    Hazard symbol(s)
    R-phrase(s)
    R22        Harmful if swallowed.
    R43        May cause sensitization by skin contact.
    R50/53        Very toxic to aquatic organisms, may cause long-term adverse effects in
    the aquatic environment.
    S-phrase(s)
    S36/37        Wear suitable protective clothing and gloves.
    S46        If swallowed, seek medical advice immediately and show this container or
    label.
    S60        This material and its container must be disposed of as hazardous waste.
    S61        Avoid release to the environment. Refer to special instructions/ Safety
    data sheets.
  Other hazards - none

Section 3. COMPOSITION/INFORMATION ON INGREDIENTS
  Substances
    Formula        : C15H17Cl2N3O2
    Molecular Weight        : 342,22 g/mol
    Component        Concentration
  Propiconazole
    CAS-No.        60207-90-1        -
    EC-No.        262-104-4
    Index-No.        613-205-00-0

Section 4. FIRST AID MEASURES
  Description of first aid measures
  General advice
    Consult a physician. Show this safety data sheet to the doctor in attendance.
  If inhaled
    If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician.
  In case of skin contact
    Wash off with soap and plenty of water. Take victim immediately to hospital. Consult a physician.
  In case of eye contact
    Flush eyes with water as a precaution.
  If swallowed
    Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.
  Most important symptoms and effects, both acute and delayed
  Indication of any immediate medical attention and special treatment needed
    no data available

Section 5. FIREFIGHTING MEASURES
  Extinguishing media
  Suitable extinguishing media
    Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.
  Special hazards arising from the substance or mixture
    Carbon oxides, nitrogen oxides (NOx), Hydrogen chloride gas
    Carbon oxides, nitrogen oxides (NOx), Hydrogen chloride gas
  Advice for firefighters
    Wear self contained breathing apparatus for fire fighting if necessary.
  Further information
    no data available

Section 6. ACCIDENTAL RELEASE MEASURES
  Personal precautions, protective equipment and emergency procedures
    Wear respiratory protection. Avoid breathing vapors, mist or gas. Ensure adequate ventilation. Evacuate
    personnel to safe areas.
  Environmental precautions
    Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the
    environment must be avoided.
  Methods and materials for containment and cleaning up
    Soak up with inert absorbent material and dispose of as hazardous waste. Keep in suitable, closed
    containers for disposal.
  Reference to other sections
    For disposal see section 13.

Section 7. HANDLING AND STORAGE
  Precautions for safe handling
    Avoid contact with skin and eyes. Avoid inhalation of vapour or mist.
  Conditions for safe storage, including any incompatibilities
    Store in cool place. Keep container tightly closed in a dry and well-ventilated place. Containers which are
    opened must be carefully resealed and kept upright to prevent leakage.
    Recommended storage temperature: 2 - 8 °C
  Specific end uses
    no data available

Section 8. EXPOSURE CONTROLS/PERSONAL PROTECTION
  Control parameters
  Components with workplace control parameters
  Exposure controls
  Appropriate engineering controls
    Avoid contact with skin, eyes and clothing. Wash hands before breaks and immediately after handling
    the product.
  Personal protective equipment
  Eye/face protection
    Face shield and safety glasses Use equipment for eye protection tested and approved under
    appropriate government standards such as NIOSH (US) or EN 166(EU).
  Skin protection
    Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique
    (without touching glove's outer surface) to avoid skin contact with this product. Dispose of
    contaminated gloves after use in accordance with applicable laws and good laboratory practices.
    Wash and dry hands.
    The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and
    the standard EN 374 derived from it.
  Body Protection
    Complete suit protecting against chemicals, The type of protective equipment must be selected
    according to the concentration and amount of the dangerous substance at the specific workplace.
  Respiratory protection
    Where risk assessment shows air-purifying respirators are appropriate use a full-face respirator
    with multi-purpose combination (US) or type ABEK (EN 14387) respirator cartridges as a backup
    to engineering controls. If the respirator is the sole means of protection, use a full-face supplied air
    respirator. Use respirators and components tested and approved under appropriate government
    standards such as NIOSH (US) or CEN (EU).

Section 9. PHYSICAL AND CHEMICAL PROPERTIES
  Information on basic physical and chemical properties
    a) Appearance        Form: liquid
    Colour: yellow
    b) Odour        no data available
    c) Odour Threshold        no data available
    d) pH        no data available
    e) Melting point/freezing        no data available
    point
    f) Initial boiling point and 180 °C at 0,129 hPa
    boiling range
    g) Flash point        no data available
    h) Evaporation rate        no data available
    i) Flammability (solid, gas) no data available
    j) Upper/lower        no data available
    flammability or
    explosive limits
    k) Vapour pressure        no data available
    l) Vapour density        no data available
    m) Relative density        no data available
    n) Water solubility        insoluble
    o) Partition coefficient: n- log Pow: 3,5
    octanol/water
    p) Autoignition        no data available
    temperature
    q) Decomposition        no data available
    temperature
    r) Viscosity        no data available
    s) Explosive properties        no data available
    t) Oxidizing properties        no data available
  Other safety information
    no data available

Section 10. STABILITY AND REACTIVITY
  Reactivity
    no data available
  Chemical stability
    no data available
  Possibility of hazardous reactions
    no data available
  Conditions to avoid
    no data available
  Incompatible materials
    Strong oxidizing agents
  Hazardous decomposition products
    Other decomposition products - no data available

Section 11. TOXICOLOGICAL INFORMATION
  Information on toxicological effects
  Acute toxicity
    LD50 Oral - rat - 1.517 mg/kg
    LC50 Inhalation - rat - 4 h - 1.264 mg/m3
    LD50 Dermal - rat - > 4.000 mg/kg
  Skin corrosion/irritation
    no data available
  Serious eye damage/eye irritation
    no data available
  Respiratory or skin sensitization
    May cause allergic skin reaction.
  Germ cell mutagenicity
    no data available
  Carcinogenicity
    IARC:        No component of this product present at levels greater than or equal to 0.1% is identified as
    probable, possible or confirmed human carcinogen by IARC.
  Reproductive toxicity
    Reproductive toxicity - rat - Oral
    Effects on Fertility: Post-implantation mortality (e.g., dead and/or resorbed implants per total number of
    implants). Effects on Embryo or Fetus: Fetotoxicity (except death, e.g., stunted fetus).
  Specific target organ toxicity - single exposure
    no data available
  Specific target organ toxicity - repeated exposure
    no data available
  Aspiration hazard
    no data available
  Potential health effects
  Inhalation
    May be fatal if inhaled. May cause respiratory tract irritation.
  Ingestion        Harmful if swallowed.
  Skin
    May be harmful if absorbed through skin. May cause skin irritation.
  Eyes        May cause eye irritation.
  Additional Information
    RTECS: XZ4620000

Section 12. ECOLOGICAL INFORMATION
  Toxicity
    Toxicity to fish        LC50 - Oncorhynchus mykiss (rainbow trout) - 0,9 - 1,2 mg/l - 96,0 h
    Toxicity to daphnia and EC50 - Daphnia magna (Water flea) - 4,8 mg/l - 48 h
    other aquatic
    invertebrates
    Toxicity to algae        EC50 - Pseudokirchneriella subcapitata (green algae) - 5 mg/l - 72 h
  Persistence and degradability
    no data available
  Bioaccumulative potential
    no data available
  Mobility in soil
    no data available
  Results of PBT and vPvB assessment
    no data available
  Other adverse effects
    Very toxic to aquatic life.

Section 13. DISPOSAL CONSIDERATIONS
  Waste treatment methods
  Product
    Offer surplus and non-recyclable solutions to a licensed disposal company.
  Contaminated packaging
    Dispose of as unused product.

Section 14. TRANSPORT INFORMATION
  UN number
    ADR/RID: 3082        IMDG: 3082        IATA: 3082
  UN proper shipping name
    ADR/RID: ENVIRONMENTALLY HAZARDOUS SUBSTANCE, LIQUID, N.O.S. (Propiconazole)
    IMDG: ENVIRONMENTALLY HAZARDOUS SUBSTANCE, LIQUID, N.O.S. (Propiconazole)
    IATA:        Environmentally hazardous substance, liquid, n.o.s. (Propiconazole)
  Transport hazard class(es)
    ADR/RID: 9        IMDG: 9        IATA: 9
  Packaging group
    ADR/RID: III        IMDG: III        IATA: III
  Environmental hazards
    ADR/RID: yes        IMDG Marine pollutant: yes        IATA: yes
  Special precautions for user
  Further information
    EHS-Mark required (ADR 2.2.9.1.10, IMDG code 2.10.3) for single packagings and combination
    packagings containing inner packagings with Dangerous Goods > 5L for liquids or > 5kg for solids.

Section 15. REGULATORY INFORMATION
    This safety datasheet complies with the requirements of Regulation (EC) No. 1907/2006.
  Safety, health and environmental regulations/legislation specific for the substance or mixture
    no data available
  Chemical Safety Assessment
    no data available

Section 16. OTHER INFORMATION
  Further information
    Copyright 2012 Co. LLC. License granted to make unlimited paper copies for internal use
    only.
    The above information is believed to be correct but does not purport to be all inclusive and shall be
    used only as a guide. The information in this document is based on the present state of our knowledge
    and is applicable to the product with regard to appropriate safety precautions. It does not represent any
    guarantee of the properties of the product. Corporation and its Affiliates shall not be held
    liable for any damage resulting from handling or from contact with the above product. See
     and/or the reverse side of invoice or packing slip for additional terms and conditions of sale.

丙环唑海关数据

中国海关编码：2934999025

概述：

2934999025 代森硫,代森环,福吗啉 ,咯菌腈等〔包括稻瘟酯,烯酰吗啉,噻菌腈,土菌灵,恶霜灵,恶霉灵〕。监管条件:S(进出口农药登记证明)。增值税率:17.0%。退税率:9.0%。最低关税:6.5%。普通关税:20.0%

申报要素：

品名, 成分含量, 用途

监管条件：

S.进出口农药登记证明

摘要/Summary：

2934999025 5,6-dihydro-3h-imidazo[2,1-c][1,2,4]dithiazole-3-thione。supervision conditions:s(import or export registration certificate for pesticides)。VAT:17.0%。tax rebate rate:9.0%。MFN tarrif:6.5%。general tariff:20.0%

丙环唑分子结构与计算化学数据

分子结构数据

1、   摩尔折射率：86.41
2、   摩尔体积（cm³/mol）：244.8
3、   等张比容（90.2K）：646.1
4、   表面张力（dyne/cm）：48.4
5、   极化率（10^-24cm³）：34.25

计算化学数据

1.疏水参数计算参考值（XlogP）:无
2.氢键供体数量:0
3.氢键受体数量:4
4.可旋转化学键数量:5
5.互变异构体数量:无
6.拓扑分子极性表面积49.2
7.重原子数量:22
8.表面电荷:0
9.复杂度:377
10.同位素原子数量:0
11.确定原子立构中心数量:0
12.不确定原子立构中心数量:2
13.确定化学键立构中心数量:0
14.不确定化学键立构中心数量:0
15.共价键单元数量:1

丙环唑表征图谱

丙环唑质谱(MS)

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丙环唑

丙环唑 制备方法及用途

制备方法

合成制备方法

用途简介

用途

丙环唑 物化性质

丙环唑 安全信息

丙环唑 毒理性

CHEMICAL IDENTIFICATION

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

丙环唑 MSDS

丙环唑 海关数据

中国海关编码：2934999025

丙环唑 分子结构与计算化学数据

分子结构数据

计算化学数据

丙环唑 表征图谱

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丙环唑制备方法及用途

丙环唑物化性质

丙环唑安全信息

丙环唑毒理性

丙环唑海关数据

丙环唑分子结构与计算化学数据

丙环唑表征图谱