丁硫克百威,55285-14-8，生产厂家，价格-洛克化工网移动版

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制备方法及用途

物化性质

安全信息

毒理性

MSDS

结构与计算化学

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丁硫克百威

中文名称：: 丁硫克百威

中文别名：: 丁硫克百威;
好安威;
丁硫威;
2,3-二氢-2,2-二甲基苯并呋喃-7-基 (二丁基氨基硫)N-甲基氨基甲酸酯;
2,3-二氢-2,2-二甲基苯并呋喃-7-基(二丁基氨基硫)甲基氨基甲酸酯;
丁呋丹;
好年冬

英文名称：: carbosulfan

英文别名：: carbosulfan;
MARSHAL;
Carbosulfan;
Versal;
BRIGHT;
2,3-dihydro-2,2-dimethylbenzofuran-7-yl (dibutylaminothio)methylcarbamate;
AMITAGE;
DBSC;
Posse;
marshall;
Sheriff;
2,3-dihydro-2,2-dimethyl-7-benzofuranyl N-[(dibutylamino)thio]-N-methylcarbamate;
2,2-dimethyl-2,3-dihydro-1-benzofuran-7-yl [(dibutylamino)sulfanyl]methylcarbamate

CAS No.：: 55285-14-8

分子式：: C20H32N2O3S

分子量：: 380.54500

精确分子量：: 380.21300

PSA：: 67.31000

MDL：: MFCD00143930

EINECS：: 259-565-9

InChI：: InChI=1/C20H32N2O3S/c1-5-7-12-22(13-8-6-2)26-15-21-19(23)24-17-11-9-10-16-14-20(3,4)25-18(16)17/h9-11H,5-8,12-15H2,1-4H3,(H,21,23)3

风险术语：: 23/25-43-50/53

SDS：: 查看

丁硫克百威制备方法及用途

制备方法

制备方法一二正丁氨基氯化硫的制备加入二正丁胺、石油醚(60～90℃),搅拌冷却至0℃,然后缓慢滴加二氯化二硫,维持0～10℃,加毕后保温反应2h,二正丁胺、二氯化二硫、硫酰氯的配比为1:0.6:0.55(mol),收率88%。丁硫克百威的合成二正丁氨基氯化硫与克百威反应,配比为1:1,反应过程加适量碱液,反应温度10～20℃。反应时间2h。反应毕加水搅拌10min,过滤,滤潭为未反应克百威,可回用。滤液分层,油层减压脱溶,收率90%。制备方法二中间体羟基化合物的合成方法见克百威。也有文献报道,由环己酮和异丁醛出发,经过叉醇醛缩合、氯化反应、芳环化反应、水解反应、闭环反应五步合成。其特点是由非芳香族化合物合成,是一种选择性很高的合成路线。中间体羟基化合物的合成方法见克百威。也有文献报道,由环己酮和异丁醛出发,经过叉醇醛缩合、氯化反应、芳环化反应、水解反应、闭环反应五步合成。其特点是由非芳香族化合物合成,是一种选择性很高的合成路线。

合成制备方法

制备方法一
二正丁氨基氯化硫的制备加入二正丁胺、石油醚（60～90℃），搅拌冷却至0℃，然后缓慢滴加二氯化二硫，维持0～10℃，加毕后保温反应2h，二正丁胺、二氯化二硫、硫酰氯的配比为1:0.6:0.55(mol)，收率88%。
丁硫克百威的合成二正丁氨基氯化硫与克百威反应，配比为1:1，反应过程加适量碱液，反应温度10～20℃。反应时间2h。反应毕加水搅拌10min，过滤，滤潭为未反应克百威，可回用。滤液分层，油层减压脱溶，收率90%。
制备方法二
中间体羟基化合物的合成方法见克百威。也有文献报道，由环己酮和异丁醛出发，经过叉醇醛缩合、氯化反应、芳环化反应、水解反应、闭环反应五步合成。其特点是由非芳香族化合物合成，是一种选择性很高的合成路线。

中间体羟基化合物的合成方法见克百威。也有文献报道，由环己酮和异丁醛出发，经过叉醇醛缩合、氯化反应、芳环化反应、水解反应、闭环反应五步合成。其特点是由非芳香族化合物合成，是一种选择性很高的合成路线。

用途简介

1.该品是呋喃丹的衍生物,具有与呋喃丹相当的杀虫活性,但其毒性比呋喃丹低得多,是一种胃毒性杀虫剂,在生物体内代谢成呋喃丹再发挥其药效作用使昆虫致死。对马铃薯绿桃蚜、黑光天牛、高染盲角蝇、地老虎等害虫均有良好的防治效果。此外,对棉花红蜘蛛、谷象、杂拟谷盗、粉纹夜蛾等也都有较好的防治。 2.具有较高的内吸性和广谱性的氨基甲酸酯类杀虫、杀螨、杀线虫剂。是克百威低毒化品种,用于防治柑橘、果树、棉花、水稻作物的蚜虫、螨、金针虫、甜菜隐食甲、马铃薯甲虫、茶微叶蝉、梨小食心虫、苹果卷叶蛾等多种害虫。

用途

1.该品是呋喃丹的衍生物，具有与呋喃丹相当的杀虫活性，但其毒性比呋喃丹低得多，是一种胃毒性杀虫剂，在生物体内代谢成呋喃丹再发挥其药效作用使昆虫致死。对马铃薯绿桃蚜、黑光天牛、高染盲角蝇、地老虎等害虫均有良好的防治效果。此外，对棉花红蜘蛛、谷象、杂拟谷盗、粉纹夜蛾等也都有较好的防治。
2.具有较高的内吸性和广谱性的氨基甲酸酯类杀虫、杀螨、杀线虫剂。是克百威低毒化品种，用于防治柑橘、果树、棉花、水稻作物的蚜虫、螨、金针虫、甜菜隐食甲、马铃薯甲虫、茶微叶蝉、梨小食心虫、苹果卷叶蛾等多种害虫。

丁硫克百威物化性质

外观与性状：
黏的棕色液体

密度：
1.099 g/cm3

沸点：
462.5ºC at 760 mmHg

闪点：
96 °C

折射率：
1.536

存储条件/存储方法：
库房通风低温干燥,与食品原料分开储运

稳定性相关：

如果遵照规格使用和储存则不会分解，未有已知危险反应


其它信息：

1.       性状：未确定
2.       密度（g/mL,25ºC）：未确定
3.       相对蒸汽密度（g/mL,空气=1）：未确定
4.       熔点（ºC）：未确定
5.       沸点（ºC）：未确定
6.       沸点（ºC，9mm hg）：未确定
7.       折射率：未确定
8.       闪点（°C）：96
9.       比旋光度（ºC）：未确定
10.    自燃点或引燃温度（ºC）：未确定
11.    蒸气压（kPa,25ºC）：未确定
12.    饱和蒸气压（kPa,60ºC）：未确定
13.    燃烧热（KJ/mol）：未确定
14.    临界温度（ºC）：未确定
15.    临界压力（KPa）：未确定
16.    油水（辛醇/水）分配系数的对数值：未确定
17.    爆炸上限（%,V/V）：未确定
18.    爆炸下限（%,V/V）：未确定
19.    溶解性：未确定

丁硫克百威安全信息

包装等级：
III

风险类别：
6.1(b)

危险类别码：
R23/25;R43;R50/53

安全说明：
S24-S37-S38-S45-S60-S61

RTECS号：
EZ3815000

安全标志：
S24:避免接触皮肤。
S37:使用合适的防护手套。
S38:在通风不良的场所，佩戴合适的呼吸装置。
S45:出现意外或者感到不适，立刻到医生那里寻求帮助（最好带去产品容器标签）。
S60:本物质残余物和容器必须作为危险废物处理。
S61:避免排放到环境中。参考专门的说明/安全数据表。

危险标志：
T:Toxic

丁硫克百威毒理性

CHEMICAL IDENTIFICATION

RTECS NUMBER :
EZ3815000

CHEMICAL NAME :
Carbamic acid, ((dibutylamino)thio)methyl-, 2,2-dimethyl-2,3-dihydro-7-benzofuranyl ester

CAS REGISTRY NUMBER :
55285-14-8

LAST UPDATED :
199712

DATA ITEMS CITED :
16

MOLECULAR FORMULA :
C20-H32-N2-O3-S

MOLECULAR WEIGHT :
380.60

WISWESSER LINE NOTATION :
T56 BOT&J C1 C1 HOVN1&SN4&4
HEALTH HAZARD DATA
ACUTE TOXICITY DATA

TYPE OF TEST :
Standard Draize test

ROUTE OF EXPOSURE :
Administration onto the skin

SPECIES OBSERVED :
Rodent - rabbit

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Rodent - rat

DOSE/DURATION :
51 mg/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LC50 - Lethal concentration, 50 percent kill

ROUTE OF EXPOSURE :
Inhalation

SPECIES OBSERVED :
Rodent - rat

DOSE/DURATION :
1530 mg/m3/1H

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Administration onto the skin

SPECIES OBSERVED :
Rodent - rat

DOSE/DURATION :
>2 gm/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Rodent - mouse

DOSE/DURATION :
74 mg/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Administration onto the skin

SPECIES OBSERVED :
Rodent - rabbit

DOSE/DURATION :
>2 gm/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Bird - quail

DOSE/DURATION :
82 mg/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Bird - duck

DOSE/DURATION :
8100 ug/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :
Oral

SPECIES OBSERVED :
Bird - wild bird species

DOSE/DURATION :
26 mg/kg

TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :
Mutation test systems - not otherwise specified

TYPE OF TEST :
Cytogenetic analysis
MUTATION DATA

TEST SYSTEM :
Rodent - mouse

DOSE/DURATION :
29600 ug/kg

REFERENCE :
MUREAV Mutation Research. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1964- Volume(issue)/page/year: 345,111,1995

毒理学数据：

1、皮肤/眼睛刺激性：标准德来塞实验：兔子皮肤接触，500 μL/24HREACTION SEVERITY，强烈反应；

生态数据：

对水是稍微有危害的不要让未稀释或大量的产品接触地下水、水道或者污水系统，若无政府许可，勿将材料排入周围环境。

丁硫克百威 MSDS

SECTION 1: Identification of the substance/mixture and of the company/undertaking
  Product identifiers
    Product name        : Carbosulfan
    REACH No.        : A registration number is not available for this substance as the substance
    or its uses are exempted from registration, the annual tonnage does not
    require a registration or the registration is envisaged for a later
    registration deadline.
    CAS-No.        : 55285-14-8
  Relevant identified uses of the substance or mixture and uses advised against
    Identified uses        : Laboratory chemicals, Manufacture of substances



SECTION 2: Hazards identification
  Classification of the substance or mixture
  Classification according to Regulation (EC) No 1272/2008
    Acute toxicity, Oral (Category 3), H301
    Acute toxicity, Inhalation (Category 2), H330
    Skin sensitisation (Category 1), H317
    Acute aquatic toxicity (Category 1), H400
    Chronic aquatic toxicity (Category 1), H410
    For the full text of the H-Statements mentioned in this Section, see Section 16.
  Classification according to EU Directives 67/548/EEC or 1999/45/EC
    T Toxic        R25
    R43
    N Dangerous for the        R50/53
    environment
    T+ Very toxic        R26
    For the full text of the R-phrases mentioned in this Section, see Section 16.
  Label elements
  Labelling according Regulation (EC) No 1272/2008
    Pictogram
    Signal word        Danger
    Hazard statement(s)
    H301        Toxic if swallowed.
    H317        May cause an allergic skin reaction.
    H330        Fatal if inhaled.
    H410        Very toxic to aquatic life with long lasting effects.
    Precautionary statement(s)
    P260        Do not breathe dust/ fume/ gas/ mist/ vapours/ spray.
    P273        Avoid release to the environment.
    P280        Wear protective gloves.
    P284        Wear respiratory protection.
    P301 + P310        IF SWALLOWED: Immediately call a POISON CENTER or doctor/
    physician.
    P310        Immediately call a POISON CENTER or doctor/ physician.
    Supplemental Hazard        none
    Statements
  Other hazards - none

SECTION 3: Composition/information on ingredients
    Formula        : C20H32N2O3S
    Molecular Weight        : 380,5 g/mol
  Hazardous ingredients according to Regulation (EC) No 1272/2008
    Component        Classification        Concentration
  Carbosulfan
    CAS-No.        55285-14-8        Acute Tox. 3; Acute Tox. 2;        <= 100 %
    EC-No.        259-565-9        Skin Sens. 1; Aquatic Acute 1;
    Index-No.        006-084-00-5        Aquatic Chronic 1; H301,
    H317, H330, H410
  Hazardous ingredients according to Directive 1999/45/EC
    Component        Classification        Concentration
  Carbosulfan
    CAS-No.        55285-14-8        T+, N, R25 - R26 - R43 -        <= 100 %
    EC-No.        259-565-9        R50/53
    Index-No.        006-084-00-5
    For the full text of the H-Statements and R-Phrases mentioned in this Section, see Section 16

SECTION 4: First aid measures
  Description of first aid measures
  General advice
    Consult a physician. Show this safety data sheet to the doctor in attendance.
  If inhaled
    If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician.
  In case of skin contact
    Wash off with soap and plenty of water. Take victim immediately to hospital. Consult a physician.
  In case of eye contact
    Flush eyes with water as a precaution.
  If swallowed
    Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.
  Most important symptoms and effects, both acute and delayed
    The most important known symptoms and effects are described in the labelling (see section 2.2) and/or in
    section 11
  Indication of any immediate medical attention and special treatment needed
    no data available

SECTION 5: Firefighting measures
  Extinguishing media
  Suitable extinguishing media
    Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.
  Special hazards arising from the substance or mixture
    Carbon oxides, nitrogen oxides (NOx), Sulphur oxides
  Advice for firefighters
    Wear self contained breathing apparatus for fire fighting if necessary.
  Further information
    no data available

SECTION 6: Accidental release measures
  Personal precautions, protective equipment and emergency procedures
    Wear respiratory protection. Avoid breathing vapours, mist or gas. Ensure adequate ventilation.
    Evacuate personnel to safe areas.
    For personal protection see section 8.
  Environmental precautions
    Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the
    environment must be avoided.
  Methods and materials for containment and cleaning up
    Soak up with inert absorbent material and dispose of as hazardous waste. Keep in suitable, closed
    containers for disposal.
  Reference to other sections
    For disposal see section 13.

SECTION 7: Handling and storage
  Precautions for safe handling
    Avoid contact with skin and eyes. Avoid inhalation of vapour or mist.
    For precautions see section 2.2.
  Conditions for safe storage, including any incompatibilities
    Store in cool place. Keep container tightly closed in a dry and well-ventilated place. Containers which are
    opened must be carefully resealed and kept upright to prevent leakage.
  Specific end use(s)
    Apart from the uses mentioned in section 1.2 no other specific uses are stipulated

SECTION 8: Exposure controls/personal protection
  Control parameters
  Components with workplace control parameters
  Exposure controls
  Appropriate engineering controls
    Avoid contact with skin, eyes and clothing. Wash hands before breaks and immediately after handling
    the product.
  Personal protective equipment
  Eye/face protection
    Face shield and safety glasses Use equipment for eye protection tested and approved under
    appropriate government standards such as NIOSH (US) or EN 166(EU).
  Skin protection
    Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique
    (without touching glove's outer surface) to avoid skin contact with this product. Dispose of
    contaminated gloves after use in accordance with applicable laws and good laboratory practices.
    Wash and dry hands.
    The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and
    the standard EN 374 derived from it.
  Body Protection
    Complete suit protecting against chemicals, The type of protective equipment must be selected
    according to the concentration and amount of the dangerous substance at the specific workplace.
  Respiratory protection
    Where risk assessment shows air-purifying respirators are appropriate use a full-face respirator
    with multi-purpose combination (US) or type ABEK (EN 14387) respirator cartridges as a backup
    to engineering controls. If the respirator is the sole means of protection, use a full-face supplied air
    respirator. Use respirators and components tested and approved under appropriate government
    standards such as NIOSH (US) or CEN (EU).
  Control of environmental exposure
    Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into
    the environment must be avoided.

SECTION 9: Physical and chemical properties
  Information on basic physical and chemical properties
    a) Appearance        Form: liquid
    b) Odour        no data available
    c) Odour Threshold        no data available
    d) pH        no data available
    e) Melting point/freezing        no data available
    point
    f) Initial boiling point and no data available
    boiling range
    g) Flash point        96 °C - closed cup
    h) Evapouration rate        no data available
    i) Flammability (solid, gas) no data available
    j) Upper/lower        no data available
    flammability or
    explosive limits
    k) Vapour pressure        0,00 hPa at 20 °C
    l) Vapour density        no data available
    m) Relative density        1,056 g/cm3
    n) Water solubility        insoluble
    o) Partition coefficient: n- no data available
    octanol/water
    p) Auto-ignition        no data available
    temperature
    q) Decomposition        no data available
    temperature
    r) Viscosity        no data available
    s) Explosive properties        no data available
    t) Oxidizing properties        no data available
  Other safety information
    no data available

SECTION 10: Stability and reactivity
  Reactivity
    no data available
  Chemical stability
    Stable under recommended storage conditions.
  Possibility of hazardous reactions
    no data available
  Conditions to avoid
    no data available
  Incompatible materials
    Strong oxidizing agents
  Hazardous decomposition products
    Other decomposition products - no data available
    In the event of fire: see section 5

SECTION 11: Toxicological information
  Information on toxicological effects
  Acute toxicity
    LD50 Oral - rat - 51 mg/kg
    LC50 Inhalation - rat - 1 h - 1.530 mg/m3
    LD50 Dermal - rabbit - > 2.000 mg/kg
  Skin corrosion/irritation
    Skin - rabbit
    Result: Mild skin irritation
  Serious eye damage/eye irritation
    no data available
  Respiratory or skin sensitisation
    Causes sensitisation.
  Germ cell mutagenicity
    Human
    lymphocyte
    Cytogenetic analysis
    Human
    lymphocyte
    Other mutation test systems
    rat
    Cytogenetic analysis
    mouse
    Micronucleus test
  Carcinogenicity
    IARC:        No component of this product present at levels greater than or equal to 0.1% is identified as
    probable, possible or confirmed human carcinogen by IARC.
  Reproductive toxicity
    no data available
  Specific target organ toxicity - single exposure
    no data available
  Specific target organ toxicity - repeated exposure
    no data available
  Aspiration hazard
    no data available
  Additional Information
    RTECS: Not available

SECTION 12: Ecological information
  Toxicity
    Toxicity to fish        LC50 - Pollimyrus isidori - 0,071 mg/l - 72,0 h
  Persistence and degradability
    no data available
  Bioaccumulative potential
    no data available
  Mobility in soil
    no data available
  Results of PBT and vPvB assessment
    PBT/vPvB assessment not available as chemical safety assessment not required/not conducted
  Other adverse effects
    Very toxic to aquatic life.

SECTION 13: Disposal considerations
  Waste treatment methods
  Product
    Offer surplus and non-recyclable solutions to a licensed disposal company.
  Contaminated packaging
    Dispose of as unused product.

SECTION 14: Transport information
  UN number
    ADR/RID: 2810        IMDG: 2810        IATA: 2810
  UN proper shipping name
    ADR/RID: TOXIC LIQUID, ORGANIC, N.O.S. (Carbosulfan)
    IMDG: TOXIC LIQUID, ORGANIC, N.O.S. (Carbosulfan)
    IATA:        Toxic liquid, organic, n.o.s. (Carbosulfan)
  Transport hazard class(es)
    ADR/RID: 6.1        IMDG: 6.1        IATA: 6.1
  Packaging group
    ADR/RID: III        IMDG: III        IATA: III
  Environmental hazards
    ADR/RID: yes        IMDG Marine pollutant: yes        IATA: no
  Special precautions for user
    no data available

SECTION 15: Regulatory information
    This safety datasheet complies with the requirements of Regulation (EC) No. 1907/2006.
  Safety, health and environmental regulations/legislation specific for the substance or mixture
    no data available
  Chemical Safety Assessment
    For this product a chemical safety assessment was not carried out

SECTION 16: Other information
  Full text of H-Statements referred to under sections 2 and 3.
    Acute Tox.        Acute toxicity
    Aquatic Acute        Acute aquatic toxicity
    Aquatic Chronic        Chronic aquatic toxicity
    H301        Toxic if swallowed.
    H317        May cause an allergic skin reaction.
    H330        Fatal if inhaled.
    H400        Very toxic to aquatic life.
    H410        Very toxic to aquatic life with long lasting effects.
  Full text of R-phrases referred to under sections 2 and 3
    N        Dangerous for the environment
    T+        Very toxic
    R25        Toxic if swallowed.
    R26        Very toxic by inhalation.
    R43        May cause sensitisation by skin contact.
    R50/53        Very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic
    environment.
  Further information
    Copyright 2014 Co. LLC. License granted to make unlimited paper copies for internal use
    only.
    The above information is believed to be correct but does not purport to be all inclusive and shall be
    used only as a guide. The information in this document is based on the present state of our knowledge
    and is applicable to the product with regard to appropriate safety precautions. It does not represent any
    guarantee of the properties of the product. Corporation and its Affiliates shall not be held
    liable for any damage resulting from handling or from contact with the above product. See
     and/or the reverse side of invoice or packing slip for additional terms and conditions of sale.

丁硫克百威分子结构与计算化学数据

计算化学数据

1.疏水参数计算参考值（XlogP）:无
2.氢键供体数量:0
3.氢键受体数量:5
4.可旋转化学键数量:10
5.互变异构体数量:无
6.拓扑分子极性表面积67.3
7.重原子数量:26
8.表面电荷:0
9.复杂度:439
10.同位素原子数量:0
11.确定原子立构中心数量:0
12.不确定原子立构中心数量:0
13.确定化学键立构中心数量:0
14.不确定化学键立构中心数量:0
15.共价键单元数量:1

丁硫克百威上游产品

呋喃丹高效杀虫剂

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呋喃丹高效杀虫剂

丁硫克百威表征图谱

丁硫克百威红外图谱(IR1)

丁硫克百威质谱(MS)

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用途简介

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丁硫克百威 MSDS

丁硫克百威 分子结构与计算化学数据

计算化学数据

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丁硫克百威表征图谱